Synthesis and characterization of trans-Mo(CO)4(p-C5NH4SO3Na)2

Suárez B., Trino; Fontal, Bernardo; Zambrano, Ghery; Reyes, Marisela del C.; Bellandi, Fernando; Contreras, Ricardo Rafael; Díaz, Juan C.; Cancines, Pedro I.; Fonseca V., Yuraima J.; Romero C., Isolda

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Fecha

2008-03-12

Autor

Suárez B., Trino

Fontal, Bernardo

Zambrano, Ghery

Reyes, Marisela del C.

Bellandi, Fernando

Contreras, Ricardo Rafael

Díaz, Juan C.

Cancines, Pedro I.

Fonseca V., Yuraima J.

Romero C., Isolda

Palabras Clave

Molybdenum, Pyridine-p-sulphonate, Carbonyl complexes

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Resumen

Reaction between Mo(CO)6 and p-C5NH4SO3Na (1:2 (Mo: p-C5NH4SO3Na) stoichiometric ratio) gave the trans-Mo(CO)4(p-C5NH4SO3Na)2 complex, (1), in 80% yield. Complex (1) has been characterized by FTIR, 1H and 13C NMR spectroscopy. Complex (1) has most likely an idealized D4h geometry with trans N-bound p-C5NH4SO3Na ligands.

URI

http://www.saber.ula.ve/handle/123456789/33631

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Información Adicional

Correo Electrónico	[email protected] [email protected], [email protected] [email protected] [email protected] [email protected] [email protected] [email protected] [email protected]
Editor	Akadémiai Kiadó, Budapest and Springer, Dordrecht
Descripción	Artículo Publicado en React.Kinet.Catal.Lett. Vol. 94, No. 1, 21−26 (2008)